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Autosampler - Model AS-1555/1555-10

autosampler_model_as1555_1555-10.jpg (12305 octets)The Model AS-1555 and AS-1555-10 are fully automatic sample injection systems enabling greater productivity and the highest possible level of precision. Sampling flexibility is unparalleled with up to 96 well positions (microplate) for laboratory automation and combinatorial chemistry. Also available is a rack for 84 micro-vials or the standard rack for 50 2 ml vials. The AS-1555/1555-10 offer 5 operating modes; normal, two methods of pre-column derivatization, dilution, and zero-sample loss injection in stand-alone mode. In the zero-sample loss mode, the sample is sandwiched between two zones of mobile phase solvent, and the entire sample volume is drawn into the loop and injected without loss.

The AS-1555 and AS-1555-10 can be easily combined with the HPLC system and the HSS-1500 software for Windows NT®. The HSS-1500 program offers full automation of your HPLC system including the autosampler, along with an audit trail and enhanced GLP compliance. The software also allows display and document maintenance information of the detector, analysis log, SOP and results of instrument validation for laboratories in regulated industries.

Features

Excellent injection reproducibility
The AS-1555/1555-10 offer operation in both fixed loop or variable volume injection modes. The reproducibility achieved in fixed loop 20 Fl injection is less than 0.2% SD with less than 0.01% sample contamination. In variable 10 Fl injections SD was less than 0.3%.

Complete flexibility
Random sample access is provided as well as random number of injections and random injection volume for each vial. Urgent samples can be given priority.

Temperature control (AS-1555-10 only)
The AS-1555-10 offers a built-in Peltier cooling and heating unit to expand the versatility of the instrument and maintain the integrity of all samples.

Non-adsorbent tubing
The AS-1555/1555-10 both use an innovative stainless steel tubing, eliminating the adsorption problem than occurs when analyzing natural samples using Teflon tubing.

Sample pretreatment capability
Air segmented sampling enables the AS-1555 and AS-1555-10 to automatically mix up to two different solvents or derivatizing reagents with the sample in a stand-alone mode. By automating the processes of derivatizations, the sample pretreatment capability saves time and improves the precision of complex chromatographic analyses.

Interfacing with the HPLC system
The AS-1555/1555-10 can be used as stand-alone module through the built-in keypad and LCD display, or integrated into a complete HPLC system with computer control. In stand-alone mode, the advanced microprocessor of the AS-1555/1555-10 offer 10 user friendly programs with 64 steps per program. The AS-1555/1555-10 can freely interact with other HPLC modules via the built-in LC-Net interface and can also easily be triggered from an external event generated by a computer or other LC modules. Full PC control is also provided when incorporated in a HPLC system with our new 3 bit HSS-1500 HPLC System control software for Windows NT®.

GLP/GMP compliance
The AS-1555/1555-10 were designed keeping GLP/GMP compliance in mind. Various GLP/GMP parameters including serial number, number of injections and number of suctions, are displayed in the LCD display. Utilizing the 32 bit HSS-1500 HPLC System control software, this GLP/GMP information is stored in a database along with an analysis log. Instrument validation can also be easily performed according to an electronic Standard Operation Procedure (SOP) provided with the HSS-1500 program. Test results of validation are recorded manually, and the results obtained are automatically compared with acceptable criteria set by user. The results can be printed for hard copy documentation along with the SOP. These various functions allow users to fully comply with GLP/GMP requirements.

Specifications
Sampling mode Partial (variable volume) or full (fixed) loop loading selectable
Number of sample 50 for standard 2 ml vials
84 for 0.6 and 0.3 ml vials
96 for microplate
Sample loop 100 Fl standard
Injection volume Variable mode 0.1 -200 Fl (standard), 1 - 2000 Fl (optional)
Fixed mode 100 Fl (standard)
Others loops 5, 10, 20, 50, 200, 500, 1000, 2000 and 5000 Fl are available as optional accessory.
Reproducibility 0.3% c.v. (Variable injection of 10 Fl)
0.2% c.v. (Fixed injection of 20 Fl)
Cross contamination 0.01% (20 Fl injection)
Sample loss 10 Fl (5 ~ 100 Fl)
Sample rack 50 sample position (Chromacol SV-2 vial)
84 sample position (Chromacol 0.3-CVG, 0.2-CTV as option
96 position microplate as option
Temperature control + 4 EC and + 37 EC by Peltier cooling unit built-in (AS-1555-10 only)
Maximum operating pressure 35 MPa
Liquid wetted materials SUS-316, fluoropolymer and glass
Operation Through interactive key operation with keypad
Operating mode Normal mode
Pre-column derivatization mode 1
Pre-column derivatization mode 2
Dilution mode
Zero-sample loss injection mode
Program function Sample nos., range, injection volume, No. of infections can be programmed in max. 64 steps. 10 such program files are avalaible and stored.
Self-diagnostics Memory (ROM,RAM), DC power supply and mechanical parts Inputs and outputs
Infection markers 3 contact closures signals
STOP OUT 1
STOP IN 1
REMOTE INJ. 1
Dimensions
AS-1555 150 (W) x 470 (D) x 307 (H) mm, approx. 12 kg
AS-1555-10 150 (W) x 470 (D) x 387 (H) mm, approx. 16 kg
Power requirements
AS-1555 150 VA
AS-1555-10 250 VA
CAT. NO. DESCRIPTION
6777-J005A Model AS-1555 Autosampler
6777-J006A Model AS-1555-10 Autosampler
6777-J004A Model AS-1550 Autosampler
6778-J002A Model PU-1580 HPLC Pump
6778-J004A Model PU-986 Semipreparative HPLC Pump
6778-J006A Model PU-987 Preparative HPLC Pump
6779-J004A Model UV-1575 UV/VIS Detector
6779-J002A Model UV-1570 UV/VIS Detector
6781-J002A Model MD-1510 Multiwavelenght UV/VIS Detector (~ 650 nm)
6781-J002A Model MD-1515 Multiwavelenght UV/VIS Detector (~ 900 nm)
6780-J002A Model FP-1520 Fluorescence Detector
6738-J002A Model UV-970M Multichannel UV Detector
6726-J002A Model RI-930 Refractive Index Detector
6734-J002A Model CL-925 Chemiluminescence Detector
6763-J002B Model CD-1595 Circular Dichroism Chiral Detector
6728-J002A Model CR-990 Chiral Polarimetric Detector
6785-J002A Model CO-1560 Column Oven
6705-H111A Cooling standard vial rack, 50 vials
6705-H112B Cooling eppendorf tube rack, 50 vials
6705-2018GA Cooling rack adaptor for 6705-H111A and 6705-H112B
6705-H113A Cooling Chromacol vial rack for 06-CTV(A), 84 vials
6705-H114A Cooling Chromacol vial rack for 03-CVG, 84 vials
6705-H119A Cooling rack adaptor for 6705-H113A and 6705-H114A
6705-H136A Cooling microplate rack including rack and acryl cover
6561-H103A Standard sample vial set, 1.5 ml. 64 btls/set, with cap and gasket
6561-H108A Standard sample vial set (amber), 1.5 ml, 64 btls/set, with cap and gasket
6561-H104A Micro sample vial set, 0.3 ml, 50btls/set, with holder, cap and gasket
0410-0039 Screw cap vial, 1.5 ml, 500 btls/set, 2-SV
0410-0041 Screw cap vial, (amber), 1.5 ml, 250 btls/set, 2-SV(A)
0410-0042 Screw cap vial (amber), 1.5 ml, 500 btls/set, 2-SV(A)
0410-0045 Screw cap vial, 1.0 ml, 500 btls/set, 1,1STVG
0410-0031 Crimp-top vial, 1.0 ml, 500 btls/set, 03-CVG
0410-0055 Crimp-top vial (amber), 0.4 ml, 500 btls/set, 06-CTV(A)
0402-0039 Crimp-top vial with septum, 1000 pcs/set